HuagongsheHuagongshe Chemistry Print Report · For research reference only
17-Bromoheptadec-6-en-1-ol → HCID 566286, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 17-Bromoheptadec-6-en-1-ol | HCID 53688827 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 566286 | HCID 566286 | 76.8% |
Reaction Steps
17-Bromoheptadec-6-en-l-ol (33.8 g) was subjected to hydrogenation in a Paar hydrogenation apparatus (50 psi initial hydrogen pressure), using ethanol as solvent and 10% palladium on charcoal as catalyst, to yield 17-bromoheptadecan-1-ol (26.1 g, 76% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05441731 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-f853bea1018e491aac81b3a4c26462e0 |
| Source note | uspto-grants-1995_08 |