HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 22921713, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Aminoacetonitrile | HCID 10901 | — |
| Reactant | 8-chlorodibenz[b,f][1,4]oxazepin-10(11H)carbonyl chloride | HCID 14975983 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22921713 | HCID 22921713 | 80.6% |
Reaction Steps
By the method of Example 18, the title compound of Example 2 (5.24 g, 17.8 mmol) in 100 mL of CH2Cl2 with molecular sieves #5A (10 g) and Et3N (2.5 mL, 18.0 mmol) was reacted with aminoacetonitrile (1.0 g, 17.8 mmol) to produce 4.5 g of the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05441950 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-d977780ef5804b0aa85a43caf42a49f1 |
| Source note | uspto-grants-1995_08 |