HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isatin → HCID 336271, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isatin | HCID 7054 | — |
| Reactant | 2H-3,1-Benzoxazine-2,4(1H)-dione, 6-nitro- | HCID 20821 | — |
| Reactant | 5-Chloroisatoic anhydride | HCID 78480 | — |
| Reactant | 5-Fluoroisatin | HCID 236566 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 336271 | HCID 336271 | 24% |
Reaction Steps
Using the procedure in Example 12, and substituting NMP for DMF, 5-nitroisatoic anhydride for 5-chloroisatoic anhydride and isatin for 5-fluoroisatin gave 495 mg (24%) of the title compound: mp 349° C. (dec); 1H NMR(CDCl3)δ 7.46-7.54 (m, 1H), 7.84-8.00 (m, 3H), 8.18-8.22 (m, 1H), 8.62-8.68 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05441955 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-49b1fedd37ac49a59624bebf2a708c17 |
| Source note | uspto-grants-1995_08 |