HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 19390815, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 19390809 | HCID 19390809 | — |
| Product | HCID 19390815 | HCID 19390815 | — |
Reaction Steps
2-[5-Benzyloxycarbonylamino-2-(4-fluorophenyl)-6-oxo-1,6-dihydropyrimidin-1-yl]-N-[3,3-difluoro-1-isopropyl-2-oxo-3-[N-(tert-butoxycarbonylmethyl)carbamoyl]propyl]acetamide. The procedure was similar to Example 1 except that a 10% hydrochloric acid wash was done. Chromatography solvent: chloroform:methanol (40:1); TLC: Rf =0.5, chloroform:methanol (40:1); MS: m/z=688(M+1). This product is also a Compound of the invention.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05441960 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-882ec56c293d4f06bfe08b1709732c8c |
| Source note | uspto-grants-1995_08 |