HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → N-formyl-(S)-isoserine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | N,O-Diformyl,(S)-Isoserine | HCID 86748890 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | N-formyl-(S)-isoserine | HCID 22855355 | — |
Reaction Steps
A stock solution of N-formyl-(S)-isoserine was prepared by stirring 20 g (124.2 mmoles) of N,O-diformyl-(S)-isoserine in a mixture of methanol (85 ml) and pyridine (15 ml, 1.5 equiv.) at room temperature for 14-16 hrs. The completion of the reaction was judged by 1HNMR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05442047 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-a4edcab0f56b4610817a2df7846508eb |
| Source note | uspto-grants-1995_08 |