Hydrochloric Acid → HCID 19389309, compound
Reaction equation
Cl.Cl.[CH3:3][NH:4][C:5]1[C:6]([O:14][CH3:15])=[C:7]([OH:13])[C:8]([O:11][CH3:12])=[CH:9][CH:10]=1>>[CH3:3][NH:4][C:5]1[C:6]([O:14][CH3:15])=[C:7]([OH:13])[C:8]([O:11][CH3:12])=[CH:9][CH:10]=1Participants
3
Procedure
On addition of ethanolic hydrogen chloride, 3-methylamino-2,6-dimethoxyphenol hydrochloride is precipitated, which product is recrystallized from isopropanol.
Workup
- customis precipitated
- customwhich product is recrystallized from isopropanol
Sources & evidence
- ORD record
- ord-24c647121e054346be3018fbf00452a6
- Source dataset
- uspto-grants-1995_08
- Patent number
- US05443596
Reaction notes
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