Trifluoroacetic acid → HCID 19389862, compound

Participants

Reaction Steps

To a mixture of the product of step D (215 mg, 0.40 mmol) and anisole (3 drops) was added TFA (3 mL). After standing at room temperature overnight, the solvent was removed and the residue was dissolved in EtOAc and washed with 2N Na2CO3 and brine. The organic was dried over MgSO4 and concentrated in vacuo to provide the titled compound, Rf=0.31 (20:1 CH2Cl2 /MeOH).

Provenance & Evidence