HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 131719091, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | Dicyclohexylamine | HCID 7582 | — |
| Reactant | N-[(Benzyloxy)carbonyl]-L-alanyl-L-prolyl-L-alanine | HCID 71395958 | — |
| Product | HCID 131719091 | HCID 131719091 | 19% |
Reaction Steps
This compound was prepared from Z-Ala-Pro-Ala-OH.dicydohexylamine in 19% yield by the procedure described in Example PKC1; single spot on tlc, Rf2 =0.55 (CHCl3 :MeOH=9:1); MS, m/e=447 (M+). Anal. Calcd. for C22H29O7N3.1/2 H2O: C, 57.88; H, 6.62; N, 9.21. Found: C, 57.65; H, 6.68; N, 9.17.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05444042 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-e61d35ab62384160ab1495c462cbe5c2 |
| Source note | uspto-grants-1995_08 |