HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Tetrachloride → HCID 15290414, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Tetrachloride | HCID 5943 | — |
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | HCID 19389969 | HCID 19389969 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 15290414 | HCID 15290414 | — |
Reaction Steps
To a suspension of 600 mg (0.0017 mol) of the product of Step D in 9 mL of acetonitrile was added 1.8 mL CCl4 and 264 mg (0.0026 mol) of methylamine. Then, 678 mg (0.0026 mol) of triphenylphosphine was added. The mixture was stirred at ambient temperature for 15 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05444079 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-f2fe3ff327514e048a30f6c717d25778 |
| Source note | uspto-grants-1995_08 |