HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15234843, compound → HCID 77768196, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15234843 | HCID 15234843 | — |
| Reactant | 9-Hydroxyspiro[5.5]undecane-3-carboxaldehyde | HCID 19390031 | — |
| Product | HCID 77768196 | HCID 77768196 | — |
Reaction Steps
Using the same reaction conditions described in Ex. 2 and 9-hydroxy-3-formyl-spiro[5.5]undecane (I-bc, Ex. 50) and dimethyl (2-oxo-[5H]-4-furyl)methylphosphonate (intermediate described in Ex. 2) as starting materials, the title compound (EZ)-9-hydroxy-3-(2-(2-oxo-[5H]-4-furyl)vinyl)-spiro-[5.5]undecane (I-ai) was obtained as an amorphous solid, identical to the one above described.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05444082 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-b7a3ec1f24014606a4b156366e7335a7 |
| Source note | uspto-grants-1995_08 |