Diaza-18-crown-6 → 4, 13-Bis(1-adamantylcarbonyl)-1,7,10,16-tetraoxa-4,13-diazacyclooctadecane

HRID 1757314Notes

Reaction equation

HRID 1757314 reaction equation
[O:1]1[CH2:18][CH2:17][O:16][CH2:15][CH2:14][NH:13][CH2:12][CH2:11][O:10][CH2:9][CH2:8][O:7][CH2:6][CH2:5][NH:4][CH2:3][CH2:2]1.[C:19]12([C:29](Cl)=[O:30])[CH2:28][CH:23]3[CH2:24][CH:25]([CH2:27][CH:21]([CH2:22]3)[CH2:20]1)[CH2:26]2>>[C:19]12([C:29]([N:4]3[CH2:5][CH2:6][O:7][CH2:8][CH2:9][O:10][CH2:11][CH2:12][N:13]([C:29]([C:19]45[CH2:28][CH:23]6[CH2:22][CH:21]([CH2:27][CH:25]([CH2:24]6)[CH2:26]4)[CH2:20]5)=[O:30])[CH2:14][CH2:15][O:16][CH2:17][CH2:18][O:1][CH2:2][CH2:3]3)=[O:30])[CH2:28][CH:23]3[CH2:24][CH:25]([CH2:27][CH:21]([CH2:22]3)[CH2:20]1)[CH2:26]2

Participants

3

Reactant 2

HCID 72805Diaza-18-crown-6HCID 989151-Adamantanecarbonyl chloride

Product 1

HCID 226302504, 13-Bis(1-adamantylcarbonyl)-1,7,10,16-tetraoxa-4,13-diazacyclooctadecane

Procedure

Analogously to Example 2 from 1,7,10,16-tetraoxa-4,13-diazacyclooctadecane and 1-adamantylcarbonyl chloride.

Sources & evidence

ORD record
ord-764bfac79c024237b1823186354fa5ab
Source dataset
uspto-grants-1995_08
Patent number
US05445762

Reaction notes

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