HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 19387524, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Pivaloyl chloride | HCID 62493 | — |
| Reactant | 1,4,7-Trioxa-10-azacyclododecane | HCID 545817 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19387524 | HCID 19387524 | — |
Reaction Steps
3.81 mmol of 1-aza-4,7,10-trioxacyclododecane are dissolved in 50 ml of CH2Cl2. 0.6 ml of triethylamine are added and 0.1 g of DMAP (=4-dimethylaminopyridine) is added as catalyst 3.82 mmol of pivalyl chloride are subsequently added, and the mixture is stirred at room temperature for 18 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05445762 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-c5136ffb43104d5ca68aaea6563c9d20 |
| Source note | uspto-grants-1995_08 |