HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trichloroacetyl chloride → HCID 19387630, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trichloroacetyl chloride | HCID 6420 | — |
| Reactant | 1,4-Cyclohexanedione | HCID 12511 | — |
| Reactant | HCID 19387600 | HCID 19387600 | — |
| Reactant | HCID 178505944 | HCID 178505944 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 19387630 | HCID 19387630 | — |
Reaction Steps
0.1 mol of 4-methylene-1-(3,4,5-trifluorophenyl)-cyclohexane (obtainable by reacting 3,4,5-trifluorophenylmagnesium bromide with the monoethylene ketal of cyclohexane-1,4-dione followed by elimination of water, hydrogenation and ketal cleavage) and 0.1 mol of trichloroacetyl chloride are reacted in accordance with Example 1B.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05445764 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-0af4a9a3c6fe46809c491cfd157ec4df |
| Source note | uspto-grants-1995_08 |