Toluene → HCID 178447807, compound

HRID 1757347Notes

Reaction equation

HRID 1757347 reaction equation
[CH2:1]([C@H:4]1[CH2:9][CH2:8][C@H:7]([CH:10]2[CH2:13][C:12]3([CH2:16][C:15](O)([C:17]4[CH:22]=[C:21]([F:23])[C:20]([F:24])=[C:19]([F:25])[CH:18]=4)[CH2:14]3)[CH2:11]2)[CH2:6][CH2:5]1)[CH2:2][CH3:3].C1(C)C=CC=CC=1.C1(C)C=CC(S(O)(=O)=O)=CC=1>O>[CH2:1]([C@H:4]1[CH2:5][CH2:6][C@H:7]([CH:10]2[CH2:11][C:12]3([CH2:16][C:15]([C:17]4[CH:18]=[C:19]([F:25])[C:20]([F:24])=[C:21]([F:23])[CH:22]=4)=[CH:14]3)[CH2:13]2)[CH2:8][CH2:9]1)[CH2:2][CH3:3]

Participants

5

Reactant 3

HCID 1140TolueneHCID 6101p-Toluenesulfonic acidHCID 178447806HCID 178447806, compound

Product 1

HCID 178447807HCID 178447807, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A mixture of 12 mmol of 4F, 100 ml of toluene and 0.5 g of p-toluenesulfonic acid is heated on a water separator for 10 hours. After conventional work-up the product is obtained, which is processed further without purification.

Workup

  1. customAfter conventional work-up the product is obtained
  2. customwhich is processed further without purification

Sources & evidence

ORD record
ord-e2df4ac376ae4fc08ab08dd7b781bf47
Source dataset
uspto-grants-1995_08
Patent number
US05445764

Reaction notes

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