HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromomethyl 4-methoxyphenyl ketone → HCID 15388729, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromomethyl 4-methoxyphenyl ketone | HCID 4965 | — |
| Reactant | 2-(Pyridin-4-yl)-4H-1,3,4-thiadiazin-5(6H)-one | HCID 23371623 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15388729 | HCID 15388729 | — |
Reaction Steps
2-(4-Pyridyl)-4H,6H-1,3,4-thiadiazin-5-one (1.88 g, 9.74 mmol) and 4'-methoxyphenacyl bromide (2.23 g, 9.74 mmol) were dissolved in absolute ethanol (40 ml) and stirred at room temperature for one day. The resultingprecipitate was collected by filtration and washed with absolute ethanol toobtain the titled compound (3.84g) as yellow powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05446042 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-992470f3a70b4544bb6cc068554aca8a |
| Source note | uspto-grants-1995_08 |