HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 19388025, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 19388029 | HCID 19388029 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 19388025 | HCID 19388025 | — |
Reaction Steps
The desired compound was prepared by addition of a solution in THF of 4-hydroxy-4-[3-(tetrahydropyran- 2-yloxy)-trans-prop-1-enyl]tetrahydro-pyran, prepared as in step 2, to a suspension of NaH in THF, followed by alkylation of the resulting anion with methyl iodide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05446062 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-8d74aeb4e9614383a6908efb1a4a44bd |
| Source note | uspto-grants-1995_08 |