HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 19388006, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Methyl Vanillate | HCID 19844 | — |
| Reactant | 1-Adamantanol | HCID 64152 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19388006 | HCID 19388006 | — |
Reaction Steps
12.37 g (68 mM) of methyl 3-methoxy-4-hydroxybenzoate in 150 ml of dichloromethane are treated with 10.33 g (68 mM) of adamantanol and 3.72 ml of concentrated sulphuric acid under the conditions described in Example 9(a). After the same treatment, there are isolated 20.3 g (94.5%) of the expected derivative, of melting point 179° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05446059 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-661a63432371454181f8bffd35505c4e |
| Source note | uspto-grants-1995_08 |