Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetamide | HCID 178 | — |
| Reactant | Phosphorus oxide (P4O10) | HCID 14812 | — |
| Reactant | HCID 19388141 | HCID 19388141 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 9797961 | HCID 9797961 | 63% |
Reaction Steps
1-[3-[2-(4-chlorophenylsulphonylamino)-ethyl]-phenoxy]-2-cyanoethane, m.p. 90°-93° C. which can be prepared by heating to 110° C. for 5 hours s mixture of 3-[2-[4-chlorophenylsulphonylamino)-ethyl]-phenoxy]-acetamide (1 mol), P2O5 (2 mol) and toluene. Yield 63% of theory; m.p. 94° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05446065 |
|---|
| Source dataset | uspto-grants-1995_08 |
|---|
| ORD ID | ord-d38c6f0a77094393931c8383c4561915 |
|---|
| Source note | uspto-grants-1995_08 |
|---|
