HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalic acid dihydrate → HCID 19388558, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalic acid dihydrate | HCID 61373 | — |
| Reactant | HCID 10826712 | HCID 10826712 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Diethyl ether ethanol | HCID 21585056 | — |
| Product | HCID 19388558 | HCID 19388558 | — |
Reaction Steps
16.90 Grammes (60.0 mmoles) of 6-chloro-3-[2-(diethylamino)ethyl]-2,3-dihydro-4(1H)-quinazolinone are dissolved in 25 ml of ethyl alcohol, to which, at the temperature of 4° C., 170 ml of a solution containing 8.32 grammes (66.0 mmoles) of dihydrate oxalic acid in a mixture of ethyl ether-ethyl alcohol in the ratio 5:1 are added.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05446152 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-6a4a6ce3ec274e158ff7eba2c7986974 |
| Source note | uspto-grants-1995_08 |