Oxalic acid dihydrate → HCID 19388576, compound

Participants

Reaction Steps

763 Milligrammes (6.1 mmoles) of dihydrate oxalic acid dissolved in 20 ml of a mixture of ethyl ether-ethyl alcohol in a ratio of 5:1 are added to 2.00 grammes (6.1 mmoles) of 1-benzyl-6-chloro-3-[2-(diethylamino)ethyl]-2,3-dihydro-4(1H)-quinazolinone and the product, which immediately crystallizes, is recovered through filtration with a yield of 50%. The product obtained has the following chemical-physical characteristics:

Provenance & Evidence