HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 22071835, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 2-Hydroxy-1,2,3-propanetricarboxylic acid hydrate (1:1) | HCID 22230 | — |
| Reactant | HCID 10619632 | HCID 10619632 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22071835 | HCID 22071835 | — |
Reaction Steps
1.00 Gramme (2.7 mmoles) of 6-chloro-1-cyclohexylmethyl-3-[2(diethylamino)ethyl]-2,3-dihydro-4(1H)-quinazolinone, dissolved in 10 ml of ethyl alcohol is joined, in agitation andat the temperature of 4° C., by 10 ml of a solution of ethyl ether and ethyl alcohol in a ratio of 5:1 containing 668 milligrammes (3.2 mmoles) of monohydrate citric acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05446152 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-4d39430d316e4efcbd005282d967764f |
| Source note | uspto-grants-1995_08 |