HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 57075905, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Ethyl butyrate | HCID 7762 | — |
| Product | HCID 57075905 | HCID 57075905 | — |
Reaction Steps
In a distillation apparatus, 86 g of t-butylaminal ester and 87 g of ethyl butyrate in 100 ml of DMF were heated so that the alcohol distilled off slowly. Distillation of the product gave 73.8 g of ethyl β-dimethylamino-2ethylacrylate, corresponding to 87.3% of the theoretical yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05446192 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-b650e03136a84f07b11ccb9db2ffbf7d |
| Source note | uspto-grants-1995_08 |