1-Bromodecane → HCID 53658819, compound

HRID 1757789Notes

Reaction equation

[N+:1]([C:4]1[CH:5]=[C:6]([C:13]([OH:15])=[O:14])[CH:7]=[C:8]([CH:12]=1)[C:9]([OH:11])=[O:10])([O-:3])=[O:2].Br[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26]>>[CH2:17]([O:14][C:13]([C:6]1[CH:5]=[C:4]([N+:1]([O-:3])=[O:2])[CH:12]=[C:8]([C:9]([O:11][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26])=[O:10])[CH:7]=1)=[O:15])[CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26]

Participants

Reactant 2

HCID 81731-Bromodecane

HCID 120695-Nitroisophthalic acid

Product 1

HCID 53658819HCID 53658819, compound

Procedure

Using this procedure the reaction of 5-nitroisophthalic acid with 1-bromodecane gave 5-nitro-1,3-benzenedicarboxylic acid didecyl ester (mp 48°-50°, Anal. Calcd for C28H45NO6 : C, 68.40; H, 9.23; N, 2.85. Found: C, 67.68; H, 9.13; N, 2.86.

Sources & evidence

ORD record: ord-d029a59ece394ac79826dcdeaa266e8b
Source dataset: uspto-grants-1995_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05446189

Reaction notes

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