Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Boron trifluoride | HCID 6356 | — |
| Reactant | Methylhydroquinone | HCID 7253 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Myristic Acid | HCID 11005 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20510464 | HCID 20510464 | — |
Reaction Steps
228 g (1 mole) of myristic acid and 136 g (1.1 mole) of monomethylhydroquinone were melted together whilst stirring a 100° C. and saturated with boron trifluoride for 4 h. After being stirred for 2 h at 100° C. the mixture was poured into 3 l of water. The product formed was pulverized under water and neutralized with a solution of 110 g of sodium carbonate in 400 ml of water, suction-filtered, washed with water, dried, and recrystallized from benzine. Yield: 305 g of compound Y1a. Melting point: 83° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04371604 |
|---|
| Source dataset | uspto-grants-1983_02 |
|---|
| ORD ID | ord-db6aa7e6f24b4b88bae30000986af1d1 |
|---|
| Source note | uspto-grants-1983_02 |
|---|
