Glycol diglycidyl ether → HCID 131712953, compound

Participants

Reaction Steps

To 50 ml of n-octanol were added 5.0 g of 3,7,7,9,9-pentamethyl-1,3,8-triazaspiro[4.5]decane-2,4-dione and 1.5 g of ethylene glycol bis(2,3-epoxypropyl) ether; the mixture was then reacted as described in Example 1 to give the desired Compound No. 340 in the form of a white powder. The compound had an Rf value of 0.54 on thin-layer chromatography on silica gel developed with a 20:1:1 by volume mixture of ethyl acetate, ethanol and triethylamine.

Provenance & Evidence