HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethyl phosphite → Hosphinecarboxylic acid, dimethoxy-, 3,4-dichlorophenyl ester, oxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethyl phosphite | HCID 8472 | — |
| Reactant | 3,4-Dichlorophenyl carbonochloridate | HCID 13077890 | — |
| Product | Hosphinecarboxylic acid, dimethoxy-, 3,4-dichlorophenyl ester, oxide | HCID 512117 | — |
Reaction Steps
From 10.3 g (85 mmole) of trimethylphosphite and 13.5 g (60 mmole) of 3,4-dichlorophenyl chloroformate (100°, 2 hours). Yield 11.4 g (64%) B.p.0.04 164° C. nD20 1.5271. Solidifies to colourless crystals m.p. 58°-9° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04372894 |
| Source dataset | uspto-grants-1983_02 |
| ORD ID | ord-9bbc1da9d361477baae0a0e4d846f837 |
| Source note | uspto-grants-1983_02 |