HRID1758225

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID8472

Trimethyl phosphite

C3H9O3P

HCID13077890

未命名化合物

PRODUCTS

生成物

HCID512117

hosphinecarboxylic acid, dimethoxy-, 3,4-dichlorophenyl ester, oxide

C9H9Cl2O5P

PROCEDURE

实验过程

From 10.3 g (85 mmole) of trimethylphosphite and 13.5 g (60 mmole) of 3,4-dichlorophenyl chloroformate (100°, 2 hours). Yield 11.4 g (64%) B.p.0.04 164° C. nD20 1.5271. Solidifies to colourless crystals m.p. 58°-9° C.