HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20509898, compound → HCID 20509920, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20509898 | HCID 20509898 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20509920 | HCID 20509920 | — |
Reaction Steps
The crude aminoacetal obtained in step (c) is dissolved in 700 ml of ethanol and is hydrogenated at room temperature and at atmospheric pressure, in the presence of 3 g of palladium catalyst (10% Pd on carbon). After the catalyst is filtered off and the filtrate evaporated, the heading compound remains as an orange oil, which is converted into the hydrochloride using methanolic hydrochloric acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04372956 |
| Source dataset | uspto-grants-1983_02 |
| ORD ID | ord-8186f80460ea49798f8a047ceef94a27 |
| Source note | uspto-grants-1983_02 |