HCID 20509903, compound → HCID 20509896, compound

Participants

Reaction Steps

1.2 g of N-(2,2-dimethoxyethyl)-2-nitro-4,5-dimethoxybenzylamine are dissolved in 20 ml of ethanol, and then hydrogenated at room temperature and at normal pressure, in the presence of 300 mg of palladium catalyst (10% on carbon). After filtering off the catalyst and evaporating the filtrate, the heading compound remains as an almost colourless oil, which is used in the next stage (e) without further purification.

Provenance & Evidence