HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 62998541, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Reactant | 2'-Aminoacetophenone | HCID 11086 | — |
| Product | HCID 62998541 | HCID 62998541 | — |
Reaction Steps
25 g of o-aminoacetophenone and 40 g of p-toluene sulfonyl chloride are together dissolved in 150 ml of pyridine and are left to stand at 50°-60° for one hour. The reaction mixture is then added to 1 liter of a stirred ice-water mixture and extracted with methylene chloride after half an hour.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04372956 |
| Source dataset | uspto-grants-1983_02 |
| ORD ID | ord-f7136b19a0e7465486e325a9596f706b |
| Source note | uspto-grants-1983_02 |