HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 131712955, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 2-Methylbenzenesulfonic acid | HCID 6925 | — |
| Reactant | Aminoacetaldehyde dimethyl acetal | HCID 89728 | — |
| Reactant | HCID 62998541 | HCID 62998541 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 131712955 | HCID 131712955 | — |
Reaction Steps
33.8 g of o-tolylsulfonylaminoacetophenone, 13.7 g of aminoacetaldehyde dimethylacetal and 0.4 g of toluenesulfonic acid in 400 ml of toluene are boiled for 4 hours in a water separator and concentrated to dryness in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04372956 |
| Source dataset | uspto-grants-1983_02 |
| ORD ID | ord-1940e349f942489090c472f3e33625bf |
| Source note | uspto-grants-1983_02 |