HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → 1-Phenyl-1-propanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Acetophenone | HCID 7410 | — |
| Solvent | Isobutanol | HCID 6560 | — |
| Product | 1-Phenyl-1-propanone | HCID 7148 | — |
Reaction Steps
0.5 liter per hour of a mixture of acetophenone and a 30% strength solution of formaldehyde in isobutanol (the molar ratio of acetophenone to formaldehyde being 8:1) was reacted at 180° C., under 30 bar H2 pressure, in the apparatus, and over the catalyst, described in Example 1. The yield of propiophenone obtained was 52.8%, based on formaldehyde employed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04374274 |
| Source dataset | uspto-grants-1983_02 |
| ORD ID | ord-a6637c0541964cd1b0e5c20de561df1a |
| Source note | uspto-grants-1983_02 |