HRID1758583
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
CONDITIONS
反应条件
- 温度
- 60 °C
PROCEDURE
实验过程
There are loaded into a 100 ml glass flask, 30 grams of methyl cumyl ether (0.2 moles), 0.1 ml of boron trifluoride diethyl etherate and 9 grams of technical cumene hydroperoxide (0.05 moles) having the same composition as that used in Example 1. The mixture is heated to 60° C. with stirring and maintained at a pressure of 200 mmHg. After 30 minutes the conversion of the cumene hydroperoxide is 100% with a yield of 99.8% of dicumyl peroxide.
WORKUP
后处理
- customThere are loaded into a 100 ml glass flask
- temperaturemaintained at a pressure of 200 mmHg