HRID1758583

反应详情

EQUATION

反应方程式

HRID 1758583 的结构方程式

CONDITIONS

反应条件

温度
60 °C

PROCEDURE

实验过程

There are loaded into a 100 ml glass flask, 30 grams of methyl cumyl ether (0.2 moles), 0.1 ml of boron trifluoride diethyl etherate and 9 grams of technical cumene hydroperoxide (0.05 moles) having the same composition as that used in Example 1. The mixture is heated to 60° C. with stirring and maintained at a pressure of 200 mmHg. After 30 minutes the conversion of the cumene hydroperoxide is 100% with a yield of 99.8% of dicumyl peroxide.

WORKUP

后处理

  1. customThere are loaded into a 100 ml glass flask
  2. temperaturemaintained at a pressure of 200 mmHg