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HRID1758704

反应详情

EQUATION

反应方程式

HRID 1758704 的结构方程式

REACTANTS

反应物

2
结构：c1ccc(SCCCN2CCNCC2)cc1
HCID2195492

未命名化合物

结构：Cn1c(=O)c2c(ncn2CC2CO2)n(C)c1=O
HCID2775876

7-(2,3-epoxypropyl)theophylline

C10H12N4O3

PRODUCTS

生成物

1
结构：Cn1c(=O)c2c(ncn2CC(O)CN2CCN(CCCSc3ccccc3)CC2)n(C)c1=O
HCID54424

7-(2-Hydroxy-3-{4-[3-(phenylsulfanyl)propyl]piperazin-1-yl}propyl)-1,3-dimethyl-3,7-dihydro-1H-purine-2,6-dione

C23H32N6O3S

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

A solution of ethanol (2 liters) containing 7-(2,3-epoxypropyl)-theophylline (1 mole) and 1-(3-phenylthiopropyl)-piperazine (1 mole) is refluxed for 5 hours. The ethanol is partly removed. The reaction medium crystallizes. The resulting crystals are suction filtered and may be recrystallized from ethanol.

WORKUP

后处理

  1. temperatureis refluxed for 5 hours
  2. customThe ethanol is partly removed
  3. filtrationfiltered
  4. custommay be recrystallized from ethanol