HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-(2-Chlorophenyl)-1-methyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepin-8-amine → HCID 20508562, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-(2-Chlorophenyl)-1-methyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepin-8-amine | HCID 12562515 | — |
| Reactant | HCID 20508545 | HCID 20508545 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20508562 | HCID 20508562 | — |
Reaction Steps
A solution of [6-(o-chlorophenyl)-1-methyl-4H-s-triazolo[4,3-a][1,4]benzodiazepin-8-yl]isocyanate is prepared as described in paragraph (a) of Example 1 from 7.0 g (21.6 mmol) of 8-amino-6-(o-chlorophenyl)-1-methyl-4H-s-triazolo[4,3-a][1,4]benzodiazepine, but using methylene chloride in place of 1,2-dichloroethane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04374773 |
| Source dataset | uspto-grants-1983_02 |
| ORD ID | ord-eadfb344159a489cae91c2b254017287 |
| Source note | uspto-grants-1983_02 |