HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Acetylpyridine → 1-(3-Pyridyl)-3-(dimethylamino)-2-propen-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Acetylpyridine | HCID 9589 | — |
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Product | 1-(3-Pyridyl)-3-(dimethylamino)-2-propen-1-one | HCID 567033 | — |
Reaction Steps
In accordance with Example 1, Part A, 0.1 mole of 3-acetylpyridine was reacted under reflux with a slight excess of N,N-dimethylformamide dimethylacetal; 3-dimethylamino-1-(3-pyridyl)-2-propen-1-one was isolated as a solid, m.p. 66°-67° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04374988 |
| Source dataset | uspto-grants-1983_02 |
| ORD ID | ord-db5386161b0644728688fac5f06ff3d3 |
| Source note | uspto-grants-1983_02 |