Undecylenic Acid → HCID 86738461, compound

Participants

Reaction Steps

To a suitable flask are added 165 grams of undecylenic acid, 29 grams of toluene and 2 grams of AMC-2 catalyst (Cordova Chemical Company oil soluble chromium complex). Heat is applied to the flask and when the temperature reaches 90° C., 114 grams of allyl glycidyl ether are added over a 30 minute period while holding the temperature at 90° C. At the completion of the addition, the temperature is held at 90° C. for 3 hours and 45 minutes, at which time the acid value is 0 indicating complete reaction.

Provenance & Evidence