HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-5-(trifluoromethyl)pyridine → HCID 13023075, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-5-(trifluoromethyl)pyridine | HCID 735862 | — |
| Reactant | 2,6-Dichlorobenzoyl isocyanate | HCID 12912739 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 13023075 | HCID 13023075 | — |
Reaction Steps
A 1.1 g. portion of 2,6-dichlorobenzoyl isocyanate and 0.8 g. of 5-trifluoromethyl-2-aminopyridine were mixed in 50 ml. of ethyl acetate at ambient temperature and stirred for 18 hours. The solvent was then evaporated and the product was recrystallized from ethanol to obtain 0.2 g. of the product named above, m.p. 228°-230° C. Elemental analysis showed:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04338321 |
| Source dataset | uspto-grants-1982_07 |
| ORD ID | ord-6658c6aa6d134f4f860d92b46877d65d |
| Source note | uspto-grants-1982_07 |