HRID1758933

反应详情

EQUATION

反应方程式

HRID 1758933 的结构方程式

PROCEDURE

实验过程

A portion of 5-trifluoromethyl-2-aminopyridine is dissolved in an inert organic solvent, and to the solution is added a portion of 2,6-difluorobenzamidocarboxylic acid, 4-nitrophenyl ester. The reaction mixture is stirred at elevated temperature for a period of time, after which the reaction mixture is evaporated to dryness under vacuum, and the product named in the heading above, identical to the product of Example 1, is isolated by recrystallization.

WORKUP

后处理

  1. customafter which the reaction mixture is evaporated to dryness under vacuum
  2. customis isolated by recrystallization