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HRID1758935

反应详情

EQUATION

反应方程式

HRID 1758935 的结构方程式

REACTANTS

反应物

2
结构：Nc1ccc(Cl)cn1
HCID66174

2-Amino-5-chloropyridine

C5H5ClN2

结构：O=C(NC(=O)c1c(F)cccc1Cl)Oc1ccc([N+](=O)[O-])cc1
HCID57040980

未命名化合物

PRODUCTS

生成物

1
结构：O=C(NC(=O)c1c(F)cccc1Cl)Nc1ccc(Cl)cn1
HCID174171

Benzamide, 2-chloro-N-[[(5-chloro-2-pyridinyl)amino]carbonyl]-6-fluoro-

C13H8Cl2FN3O2

PROCEDURE

实验过程

A portion of 2-chloro-6-fluorobenzamidocarboxylic acid, 4-nitrophenyl ester, is combined with a portion of 5-chloro-2-aminopyridine in an inert organic solvent. The reaction mixture is stirred at elevated temperature for a period of time, and is then evaporated under vacuum. The product named in the heading above, identical to the product of Example 3, is isolated by recrystallization.

WORKUP

后处理

  1. customis then evaporated under vacuum
  2. customis isolated by recrystallization