HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-1-(3-chlorophenyl)ethan-1-ol → Brl 35135
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-1-(3-chlorophenyl)ethan-1-ol | HCID 3751601 | — |
| Reactant | Methyl 2-(4-(2-oxopropyl)phenoxy)acetate | HCID 13851156 | — |
| Product | Brl 35135 | HCID 122186 | — |
Reaction Steps
The compound was prepared as in Example 5 from 1-(4-carbomethoxymethoxyphenyl)propan-2-one (2.22 g) and 2-hydroxy-2-(3-chlorophenyl) ethanamine (1.71 g) and crystallised from hexane m.p. 82°-87° as a 58:42 mixture of diastereoisomers.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04338333 |
| Source dataset | uspto-grants-1982_07 |
| ORD ID | ord-e6fd09130ebc493e843ee4440ed1af39 |
| Source note | uspto-grants-1982_07 |