HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylethanolamine → HCID 20533256, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylethanolamine | HCID 1000 | — |
| Reactant | Methyl 2-(4-(2-oxopropyl)phenoxy)acetate | HCID 13851156 | — |
| Product | HCID 20533256 | HCID 20533256 | — |
Reaction Steps
The compound was prepared as in Example 1 from 1-(4-carbomethoxymethoxyphenyl)propan-2-one (4.1 g) and 2-hydroxy-2-phenylethylamine (2.53 g). The compound was purified initially by column chromatography on silica gel and crystallised as the hydrobromide salt from methanol/diethyl ether m.p. 147°-160° as a 90:10 mixture of diastereoisomers.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04338333 |
| Source dataset | uspto-grants-1982_07 |
| ORD ID | ord-9e3c2600634e46c8828858ec16f1ba63 |
| Source note | uspto-grants-1982_07 |