HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylethanolamine → N-[2-(4-(3-Carbomethoxypropoxy)phenyl)-1-methylethyl]-2-hydroxy-2-phenylethanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylethanolamine | HCID 1000 | — |
| Reactant | 1-(4-[3-Carbomethoxypropoxy]phenyl)propan-2-one | HCID 13079613 | — |
| Product | N-[2-(4-(3-Carbomethoxypropoxy)phenyl)-1-methylethyl]-2-hydroxy-2-phenylethanamine | HCID 20533267 | — |
Reaction Steps
The compound was prepared as in Example 5 from 1-(4-(3-carbomethoxypropoxy)phenyl] propan-2-one (6.0 g) and 2-hydroxy-2-phenyl ethanamine (3.29 g) and crystallised from hexane m.p. 60°-76° as a 1:1 mixture of diastereoisomers.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04338333 |
| Source dataset | uspto-grants-1982_07 |
| ORD ID | ord-43470565d5dc4c9fb84f3c06fbd772de |
| Source note | uspto-grants-1982_07 |