HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-[4-(3-Carbomethoxyprop-2-eneoxy)phenyl]propan-2-one → 1-(4-[3-Carbomethoxypropoxy]phenyl)propan-2-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-[4-(3-Carbomethoxyprop-2-eneoxy)phenyl]propan-2-one | HCID 53825375 | — |
| Edukt | HCID 178418361 | HCID 178418361 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 1-(4-[3-Carbomethoxypropoxy]phenyl)propan-2-one | HCID 13079613 | 99,2% |
Reaktionsschritte
To a solution of 1-[4-(3-carbomethoxyprop-2-eneoxy)phenyl]propan-2-one (1.1 g) in ethanol (50 ml), was added 10% Pd/C (100 mg) and the mixture hydrogenated at ambient temperature and atmospheric pressure until hydrogen uptake was complete (approx. 10 minutes). The solution was filtered, evaporated to give the title compound (1.1 g) as an oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04338333 |
| Quelldatensatz | uspto-grants-1982_07 |
| ORD ID | ord-5fe1d94af7b0417cb1bc3a573dc4aeb7 |
| Quellennotiz | uspto-grants-1982_07 |