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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1758988Erstellt: 25. Oktober 2026

1-[4-(3-Carbomethoxyprop-2-eneoxy)phenyl]propan-2-one → 1-(4-[3-Carbomethoxypropoxy]phenyl)propan-2-one

https://huagongshe.com/reaction/1758988

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt1-[4-(3-Carbomethoxyprop-2-eneoxy)phenyl]propan-2-oneHCID 53825375—
EduktHCID 178418361HCID 178418361—
KatalysatorPalladiumHCID 23938—
LösungsmittelEthanolHCID 702—
Produkt1-(4-[3-Carbomethoxypropoxy]phenyl)propan-2-oneHCID 1307961399,2%

Reaktionsschritte

To a solution of 1-[4-(3-carbomethoxyprop-2-eneoxy)phenyl]propan-2-one (1.1 g) in ethanol (50 ml), was added 10% Pd/C (100 mg) and the mixture hydrogenated at ambient temperature and atmospheric pressure until hydrogen uptake was complete (approx. 10 minutes). The solution was filtered, evaporated to give the title compound (1.1 g) as an oil.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04338333
Quelldatensatzuspto-grants-1982_07
ORD IDord-5fe1d94af7b0417cb1bc3a573dc4aeb7
Quellennotizuspto-grants-1982_07