HRID1758988

反应详情

EQUATION

反应方程式

HRID 1758988 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a solution of 1-[4-(3-carbomethoxyprop-2-eneoxy)phenyl]propan-2-one (1.1 g) in ethanol (50 ml), was added 10% Pd/C (100 mg) and the mixture hydrogenated at ambient temperature and atmospheric pressure until hydrogen uptake was complete (approx. 10 minutes). The solution was filtered, evaporated to give the title compound (1.1 g) as an oil.

WORKUP

后处理

  1. customhydrogenated at ambient temperature
  2. custom(approx. 10 minutes)
  3. filtrationThe solution was filtered
  4. customevaporated