Acetone → HCID 13068411, compound

HRID 1759142Notes

Reaction equation

HRID 1759142 reaction equation
[CH3:1][O:2][C:3]1[C:8]2[CH2:9][CH2:10][CH2:11][C:7]=2[N:6]=[C:5]([NH:12][C:13](=[N:17][S:18]([C:21]2[CH:30]=[CH:29][CH:28]=[CH:27][C:22]=2[C:23]([O:25][CH3:26])=[O:24])(=[O:20])=[O:19])SCC)[N:4]=1.CC(C)=[O:33]>>[CH3:1][O:2][C:3]1[C:8]2[CH2:9][CH2:10][CH2:11][C:7]=2[N:6]=[C:5]([NH:12][C:13]([NH:17][S:18]([C:21]2[CH:30]=[CH:29][CH:28]=[CH:27][C:22]=2[C:23]([O:25][CH3:26])=[O:24])(=[O:20])=[O:19])=[O:33])[N:4]=1

Participants

3

Reactant 2

HCID 180AcetoneHCID 70527036HCID 70527036, compound

Product 1

HCID 13068411HCID 13068411, compound

Procedure

A solution of 3.2 g of methyl 2-[[1-(6,7-dihydro-4-methoxy-5H-cyclopentapyrimidin-2-ylamino)-1-(ethylthio)methylene]aminosulfonyl]benzoate in 75 ml of acetone is treated with 3.0 g of mercuric oxide and stirred at room temperature for 3 days. The mercury salts are removed by filtration and the solvent is evaporated to yield the solid product.

Workup

  1. customThe mercury salts are removed by filtration
  2. customthe solvent is evaporated
  3. customto yield the solid product

Sources & evidence

ORD record
ord-4952a8744f874c36baa50b9e549ecce9
Source dataset
uspto-grants-1982_07
Patent number
US04339267

Reaction notes

Loading…