Chloride → 2-(Hydroxyimino)thiomorpholin-3-one

HRID 1759153Notes

Reaction equation

HRID 1759153 reaction equation
N(=S1C=C[CH2:6][C:5](=O)[NH:4]1)O.[Cl-].[OH-:11].[Na+].[NH2:13][CH:14]([SH:16])[CH3:15].C([OH:19])C>>[N:13](=[C:14]1[C:15](=[O:19])[NH:4][CH2:5][CH2:6][S:16]1)[OH:11]

Participants

6

Reactant 5

HCID 312ChlorideHCID 702EthanolHCID 14798Sodium HydroxideHCID 129159481-Aminoethane-1-thiolHCID 70546111HCID 70546111, compound

Product 1

HCID 713661032-(Hydroxyimino)thiomorpholin-3-one

Procedure

The oximino-thiazin-3-one compounds can be prepared in accordance with a method disclosed in U.S. Pat. No. 3,894,150. Ethoxycarbonylformhydroxamoyl chloride is added to a solution of sodium hydroxide, ethanol and aminoethanethiol to produce an oximino-tetrahydro-1,4-thiazin-3-one.

Sources & evidence

ORD record
ord-e84fd676020d458696170f501cc92411
Source dataset
uspto-grants-1982_07
Patent number
US04339444

Reaction notes

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