Sodium Iodide → HCID 23676571, compound

HRID 1759155Notes

Reaction equation

HRID 1759155 reaction equation
[O:1]=[C:2]([P:5](=[O:10])([O:8]C)[O:6][CH3:7])[CH2:3][CH3:4].[I-].[Na+:12]>CC(CC)=O>[O:1]=[C:2]([P:5](=[O:8])([O-:10])[O:6][CH3:7])[CH2:3][CH3:4].[Na+:12]

Participants

4

Reactant 2

HCID 5238Sodium IodideHCID 298017Dimethyl (1-oxopropyl)phosphonate

Product 1

HCID 23676571HCID 23676571, compound

Reagents, catalysts & solvents 1

HCID 6569Methyl Ethyl KetoneSolvent

Procedure

Dimethyl (1-oxopropyl)phosphonate (10.0 g, 0.060 mol) and sodium iodide (9.0 g, 0.060 mol) were dissolved in ethyl methyl ketone (160 ml) and the solution stirred and refluxed for 16 hours.

Workup

  1. temperaturerefluxed for 16 hours

Sources & evidence

ORD record
ord-4a621ecd6d9f43cea5c99165dff55a14
Source dataset
uspto-grants-1982_07
Patent number
US04339443

Reaction notes

Loading…