Sodium Iodide → HCID 23701879, compound

HRID 1759156Notes

Reaction equation

HRID 1759156 reaction equation
[C:1]([P:9](=[O:14])([O:12]C)[O:10][CH3:11])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[I-].[Na+:16]>CC(CC)=O>[C:1]([P:9](=[O:12])([O-:14])[O:10][CH3:11])(=[O:8])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1.[Na+:16]

Participants

4

Reactant 2

HCID 5238Sodium IodideHCID 256107Dimethyl benzoylphosphonate

Product 1

HCID 23701879HCID 23701879, compound

Reagents, catalysts & solvents 1

HCID 6569Methyl Ethyl KetoneSolvent

Procedure

Dimethyl benzoylphosphonate (12.8 g, 0.06 mol) and sodium iodide (9.0 g, 0.06 mol) were dissolved in ethyl methyl ketone (160 ml) and the solution stirred and refluxed for 16 hours. There was evidence of a precipitation after about 10 minutes refluxing.

Workup

  1. temperaturerefluxed for 16 hours
  2. customevidence of a precipitation after about 10 minutes
  3. temperaturerefluxing

Sources & evidence

ORD record
ord-d7b8652cdfe74f14b611d5a379f0b61f
Source dataset
uspto-grants-1982_07
Patent number
US04339443

Reaction notes

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