Sodium Iodide → HCID 86738471, compound

HRID 1759157Notes

Reaction equation

HRID 1759157 reaction equation
[O:1]=[C:2]([P:6](=[O:11])([O:9]C)[O:7][CH3:8])[CH2:3][CH2:4][CH3:5].[I-].[Na+:13]>CC(CC)=O>[O:1]=[C:2]([P:6](=[O:9])([O-:11])[O:7][CH3:8])[CH2:3][CH2:4][CH3:5].[Na+:13]

Participants

4

Reactant 2

HCID 5238Sodium IodideHCID 15685100Dimethyl butanoylphosphonate

Product 1

HCID 86738471HCID 86738471, compound

Reagents, catalysts & solvents 1

HCID 6569Methyl Ethyl KetoneSolvent

Procedure

Dimethyl (1-oxobutyl)phosphonate (10.8 g, 0.06 mol) and sodium iodide (9.0 g, 0.06 mol) were dissolved in ethyl methyl ketone (160 ml) and the solution stirred and refluxed for 16 hours.

Workup

  1. temperaturerefluxed for 16 hours

Sources & evidence

ORD record
ord-8eec13095dd74b04aca35867d2aaf433
Source dataset
uspto-grants-1982_07
Patent number
US04339443

Reaction notes

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